Experiment 1:  Identification of an Unknown Compound by Spectroscopy

• No additional information required

Experiment 2:  Addition of Gignard Reagents to Isophorone

• Glassware setup
  

• NMR of Diels-Alder adduct

• Molecular modelling and database searching information
  

Experiment 3:  Oxidation of Alcohols

• Vacuum distillation setup
  

• J. Meinwald, J. Crandall, W. E. Hymans, Org. Synth., Coll. Vol. V, p. 863. (not available online)

• E. J. Corey, J. W. Suggs, Tetrahedron Lett., 1975, 2647. (not available online)

Experiment 4:  An Introduction to Flash Column Chromatography

• W. C. Still, M. Kahn, A. Mitra, J. Org. Chem. , 1978, 43, 2923.

Experiment 5:  Preparation of bis(triphenylphosphine)copper(I) tetrahydroborate

• S. J. Lippard and D. Ucko, Inorg. Chem., 1968, 7, 1051.

• S. J. Lippard and K. M. Melmed, Inorg. Chem., 1967, 6, 2223.

Experiment 6:  Nitrosyl Complexes of Iron and Nickel

• Soxhlet extration setup
  

• M. Colapietro, A. Domenicano, L. Scaramuzza, A. Vaciago and L. Zanbonelli, J. Chem .Soc., Chem. Commun., 1967, 583. (not available online)

• ESR Spectrum (Note:  You have to take measurements off this spectrum so make sure print it at 100% size and check the scale.  If in doubt obtain a hard-copy from a demonstrator)

Experiment 7:  Nitration of Cobalt(III) Acetylacetonate

• J. P. Collman, R. L. Marshall, W.L. Young and S.D. Golby, Inorg. Chem., 1962, 1, 704 .
  

• K. Nakamoto, P. J. McCarthy, A. Ruby and A. E. Martell, J. Am. Chem. Soc., 1961, 83, 1066.

• ¹H NMR Spectrum of Co(III)acetylacetonate

• ¹H NMR Spectrum of Nitration product
  

Experiment 8:  Influence of Ligand Field Tetragonality on the Ground State Spin

• D. M. L. Goodgame and L. M. Venanzi, J. Chem. Soc., 1963, 616. (not available online)

• Operating instructions for the magnetic susceptibility balance
  

• Sample effective magnetic moment calculation

Experiment 9:  [Co(dinosar)]Cl₃:  An Encapsulation Complex Prepared by a Template Reaction

• R. J. Geve, T. W. Hambley, J. M. Harrowfield, A. M. Sargeson and M. R. Snow, J. Am. Chem. Soc., l984, 106, 5478.

• ¹H NMR Spectra of [Co(dinosar)]Cl₃

• ¹³C NMR Spectra of [Co(dinosar)]Cl₃

Experiment 10:  Anomalous Paramagnetism in some Iron(III) Chelates Studied by the Evans NMR Method

• T. H. Crawford and J. Swanson,  J. Chem. Ed., 1971, 48, 382. (not available online)

• A. H. White, R. Roper, E. Kokot,  H. Waterman and R. L. Martin, Aust. J. Chem., 1964, 17, 294. (not available online)

• A. H. Ewald, R. L. Martin, E. Sinn, and A. H. White, Inorg. Chem., 1969, 8, 1837.